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[Amps] RF insulating materials - engineered plastics

To: amps@contesting.com
Subject: [Amps] RF insulating materials - engineered plastics
From: John Lyles <jtml@losalamos.com>
Reply-to: jtml@vla.com
Date: Tue, 28 Aug 2012 00:40:48 -0600
List-post: <amps@contesting.com">mailto:amps@contesting.com>
I just finished a series of comparison tests of a handful of polymeric 
materials and blends, for use in high power VHF amplifier projects. I 
didn't test Nylon, Delrin acetal, Polyethylene or Polypropylene. What I 
did test was vigin PTFE, 25% glass + PTFE, Polystyrene (Rexolite), 
Polysulfone (Udel), Polyetherimide + Glass (ULTEM) and G7 (glass + 
silicone resin laminate). One new material that i was skeptical about 
was Duraform, a material used in 3D solid printing. All are materials 
that I have used one time or another in high power projects in my 
workplace. Each material was machined in the same shape, 1.5 inch 
diameter cylindrical puck, 0.75 inches thick. They were placed in a WT 
LaRose "Thermall" Model 9 dielectric preheater, using a single Amperex 
5868 triode at ~90 MHz. Approximate voltage across parallel plates was 
15 kV peak, and the plates were compressed against each sample, without 
air gaps. As they were inserted, all materials loaded the machine at 
roughly the same plate current. Temperature was taken with a Stanley IR 
thermometer, the point and shoot type, at 6 inches from flat surface of 
puck. By soaking them in this extreme field for 2 minutes, I was able to 
make a realistic relative comparison of their loss tangent at 90 MHz. 
This is worthhile information when designing with polymer insulators 
inside amplifiers.

Now the results, sorted in order of loss:
Material      StartTemp EndTemp  Start Ip End Ip    Comment

PTFE (Teflon)     84 degF 86 deg   210 mA  210         best
PTFE+Glass        84     98        20      205  goodmechanical
Polysulfone(UDEL) 86    188       200      200 translucent amber
PEI (ULTEM)+Glass 84    207       200      203     laminate
Polystyrene(Rexolite) 84 215      210      >300     runaway, 45 sec
G7                84     292      190      190
Duraform          84     210      200      >350    runaway, melt 10 sec

Conclusion: Virgin Teflon is the winner, as expected. If it weren't for 
the difficulty of mechanical stability and strength, there would be 
nothing else needed. But it is quite costly now, since the Japanese 
disaster. A good substitute for strength is the Teflon+Glass mixture.
UDEL and ULTEM are both great materials, and about similar in loss 
properties as medium quality dielectrics. Rexolite, widely used for 
radomes, coaxial line supports, and in cavities, has a runaway loss 
tangent property with temperature as it nears glass transition.
G7 is good for lower frequencyies, not so at VHF. Duraform is a terrible 
insulator, but great as a printable material for 3D models.

I welcome any comments or suggestions.
73
K5PRO
John
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